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Answer :
Final answer:
The most accurate way to charge a capillary tube system involves careful sample insertion, securing the tube to a thermometer for stability.
Explanation:
The most accurate method of charging a capillary tube system in a laboratory setting involves precise handling and measurement of the sample. First, the user should fill the small tube nearly half-full with the sample. Subsequently, they need to insert a capillary tube with its closed end up into this sample.
The capillary tube is then secured to a thermometer using a small rubber band, ensuring it is stable during the charging process. The LibreTexts methodology suggests loading the sample by jabbing the capillary's open end into the sample pile, followed by dropping the tube down a long hollow tube to pack the sample into the closed end.
Controlling the height of the sample in the capillary tube is crucial; typically, a height of 2-3 mm is recommended. Also, correctly applying heat until a stream of bubbles emerges at a specific rate ensures the sample is at the right temperature for analysis.
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